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Benzyl methyl ketone synthesis

The planned approach for the total synthesis of brevetoxin A5focused on a versatile endgame that would exploit the selective manipulation of tetraol 2(Scheme 1), which would derive from mixed methyl ketal 3via stereoselective reductive etherification.
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Benzylmethylketone, also known as phenyl-2-propanone occurs as a metabolite of amphetamine via oxidative deamination. It is used as an intermediate in the production of.

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step synthesis increases the synthesis by two non-productive ... unsaturated ketone is less electrophilic and therefore less reactive to ... + CH 3 OH LiOH H 2 O 2 21 The common ester protecting groups for carboxylic acids are methyl, ethyl and benzyl esters. 1:56 PM. Protecting Groups for Carboxylic Acids (Esters) Ethyl and benzyl esters are.
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(ii) Williamson's ether synthesis : The reaction involves the nucleophilic substitution of the halide ion from the alkyl halide by the alkoxide ion by S N 2 mechanism. Example : (b) 2-Propanol is a secondary alcohol. When it reacts with I 2 in NaOH, it forms a yellow ppt of iodoform but 2-methyl-2 propanol does not respond to this test.
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General procedure for the synthesis of 10 (R)-Methyl 3- (ethoxycarbonylamino)butanoate 10a: To a cold solution (0 °C) of (+)- ( R )- N -benzyl- N -α-methylbenzylamine (23.0 mL, 110 mmol, 1.1 equiv) in dry THF (280 mL) was added n -butyllithium (75.0 mL, 1.6 M in hexane, 120 mmol, 1.2 equiv) slowly under argon.
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Treatment of acetoacetic ester with 1) base, 2) methyl bromide, 3) acidic water and 4) heat will give acetone. Acetoacetatic ester can be used for synthesis of ketone. Acetoacetatic ester has an acidic alpha hydrogen and it can be substituted into an alkyl group.
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Toronto Research Chemicals 20 Martin Ross Avenue Toronto, ON Canada, M3J 2K8 International: +1 (416) 665-9696 US & Canada: +1 (800) 727-9240 Email: [email protected] TRC is a subsidiary of LGC Standards.
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Grignard reagents are our first source of carbanions (literally, "anions of carbon"). The Lewis structure of the CH 3- ion suggests that carbanions can be Lewis bases, or electron-pair donors. Grignard reagents such as methylmagnesium bromide are therefore sources of a nucleophile that can attack the + end of the C=O double bond in aldehydes.
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The most commonly employed methods of synthesis of drugs of this type are briefly described. Special emphasis is given to the Leuckart route, found to be the preferred method, in the illicit ... The reductive amination of benzyl methyl ketone is im-ForensicScienceReview • VolumeOne NumberOne • June 1989. portant [8,16], while in Sweden and.
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Market Place. tert-Butyl Methyl Ketone (CAS 75-97-8) Intermediate needed in India [ENA09890] A large pharmaceutical manufacturing and R&D company that deals in more than 5 therapeutic segments is looking for suppliers of tert-Butyl Methyl Ketone (CAS 75-97-8) Intermediate. The required quantity is 100 kg.
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Buy Quality Benzyl methyl ketone Online Phenylacetone,is an organic compound.It is a clear oil with a refractive index of 1.5168.This substance. Methyl fluoroacetate (MFA) is an extremely toxic methyl ester of fluoroacetic acid.It is a colorless, odorless liquid at room temperature. It is used as a laboratory chemical and as a rodenticide.Because of its extreme toxicity, MFA was studied for potential use as chemical weapon. The general population is not likely to be exposed to methyl fluoroacetate. Going green! The rhodium(III)‐catalyzed annulation of aryl ketone O‐methyl oximes with isocyanates for the synthesis of 3‐methyleneisoindolin‐1‐ones is reported (see scheme). This reaction exhibits high regioselectivity, functional‐group tolerance, and broad substrate scope, without the use of additives or production of environmentally hazardous waste. Product name: Raspberry Ketone Glucoside Other Name: RKG; raspberry ketone glucoside ketone; 4-[4-(beta-D-Glucopyranosyloxy)phenyl]-2-butanone INCI Name: RASPBERRYKETONE GLUCOSIDE Molecular Formula: C16H22O7 Molecular Weight: 326.34 Appearance: White crystalline powder;Well soluble in water Purity: 99% CAS NO.: 38963-94-9 EINECS No.:.

Benzyl methyl ketone, Benzyl Methyl Ketone sales usa, benzyl methyl ketone synthesis, buy benzyl methyl ketone worldwide shipping, Buy phenylacetone 99.34%, Buy phenylacetone 99.34% purity, how to.

These methyl ketones and an open chain congener, benzyl levulinate, were inert toward m-chloroperbenzoic acid. The cis-isomer and benzyl levulinate underwent normal Baeyer-Villiger. An efficient and green route of C–C bond formation was disclosed to construct 2,3-diaryl-1,4-diketones from α-methylene ketones by the catalysis of tetrabutylammonium iodide (TBAI) with tert-butyl hydroperoxide (TBHP) as an oxidant in water. This reaction affords the desired products in good to excellent yields from readily available materials, with a broad. E cient Synthesis of 1-Alkoxycarbonyl-Methyl-2-Alkylpyrroles...,R. A. GADZHILI, et al., Potassium salt of 2-(2-ethyl-1H-pyrrol-1-yl)acetic acid 11b To a solution of 0.05 mol of potassium hydroxide in 100 ml of methyl or ethyl alcohol at 55-60 Cwas added dropwise 0.05 mol of methyl 2-(2-ethyl-1H-pyrrol-1-yl)acetate 3b dissolved in 25 ml of alcohol.The.

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Buy high quality Alpha Methyl Naphtyl Ketone online at the best price. Our office is based in Mumbai, Maharashtra (India). Some of our important markets are Hyderabad, Pune, Saharanpur, Gorakhpur, Bikaner, Solapur, Vijayawada, Jabalpur, Kota. For more details, contact us at +918045477201. . It might be synthesized by the reaction of benzaldehyde and nitroethane inside seeing a basic driving force. In this reaction, the base deprotonates nitroethane to outline a resonation offset anion. This anion nucleophilically adds to the aldehyde confining a beta nitro alcohol, which is thusly got dried out to yield the nitroalkene.

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Treatment of acetoacetic ester with 1) base, 2) methyl bromide, 3) acidic water and 4) heat will give acetone. Acetoacetatic ester can be used for synthesis of ketone. Acetoacetatic ester has an acidic alpha hydrogen and it can be substituted into an alkyl group.

  • Unless listed in another schedule, any material, compound, mixture, or preparation which contains any quantity of the following substances: (1) Immediate precursor to amphetamine and methamphetamine: (A) Phenylacetone, phenyl-2-propanone(P2P), benzyl methyl ketone, methyl benzyl ketone;. 5-benzyl-, 7-benzyl-, and 5,7-dibenzylindolizidinone amino acids 2-4 were stereoselectively synthesized via efficient reaction sequences featuring the alkylation of di-tert-butyl alpha,omega-di-[N-(PhF)amino]azelate delta-ketone 5. A variety of alkyl halides were readily added to the enolate of ketone 5 to. Normally, anything that can generate a carbocation shows, for example, a Friedel-Crafts alkylation reaction. I wanted to know if this reaction is also possible: taking an aldehyde or a ketone with an acid, which will protonate the oxygen atom and generate a carbocation - followed by electrophilic attack on benzene.

  • Methyl 2-pyridyl ketone: 3D: Download 3D: Methyl 2-pyridyl ketone is one of the main components in the odor of popcorn. One of the ironies of organic chemistry is that while pyridine itself smells like something that died a long time ago, hanging a ketone group off the pyridine ring produces the pleasant, mouth-watering odor of popcorn. Pyrazine. These catalysts showed excellent reactivity towards alkylation of carbonyl compounds with low catalyst loading (0.01 mol %) and were found to be highly effective in synthesizing the quinoline derivatives with catalyst loading of as low as 0.01 mol %. The catalytic potential for gram-scale synthesis was also examined. Abstract. In an attempt to synthesize carvotacetone analogues, new 3-O-benzyl-carvotacetone (10) and previously reported 3-hydroxy-2-isopropyl-5-methyl-p-benzoquinone (11) were synthesized from piperitone (7).In this work, we describe the synthesis of 10 and other analogues from 7.Luche reduction of 7 to cis-piperitol (8), followed by benzylation yielded 3-O-benzyl-piperitol (9).

It is well known that benzyl methyl ketone (BMK) can be employed as a precursor in the synthesis of amphetamine. Similarly, it is reasonable to assume that ketone precursors may potentially be utilized in the clandestine synthesis of BDF and its homologues. The synthetic compound was loaded onto discs with concentrations of 0.2, 0.3, 0.4 and 0.5 µg mL −1 and air-dried. The dry discs were placed on the inoculated Mueller-Hinton agar plates and incubated at 310 K for 48 h. A penicillin disc (10 µg per disc) was used as the standard. A disc of 150 µl of DMSO served as the control.

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The odor threshold for methyl ethyl ketone is 5.4 parts per million (ppm), with an acetone-like odor reported. (3) The chemical formula for methyl ethyl ketone is C4H8O and the molecular weight is 72.10 g/mol. (7,9) The vapor pressure for methyl ethyl ketone is 95.1 mm Hg at 25 °C, and it has a log octanol/water partition.

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  • General procedure for synthesis of 2-(2-benzyl-1H-benzo[d]imidazol-1-yl) acetohydraz- ones (4-8) Benzimidazole acid hydrazide 3 (5 mmol) was dissolved in a 20 mL ethanol and five drops of acetic acid. Later substituted aryl methyl ketone or benzaldehyde (10 mmole) was added to the mixture and the contents were heated under reflux (6-8 h).

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Phenylacetone is an organic compound with the chemical formula C 6 H 5 CH 2 COCH 3. It is a colorless oil that is soluble in organic solvents. This substance is used in the manufacture of methamphetamine and amphetamine, where it is commonly known as P2P.

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Reaction of cyclopentadiene with methyl vinyl ketone. In this reaction only two possible diastereoisomers can be formed - exo and endo. We can work out which is the endo product using the method described, and this turns out to be the product with the carbonyl group on the opposite side to the CH 2 bridge. J. Sauer, Angew. In a batch reactor, the synthesis of benzyl methyl ether from benzyl alcohol and methanol in high-temperature carbonic water was investigated. When benzyl alcohol was combined with methanol under supercritical conditions at 573 K, no benzyl methyl ether was produced. The treatment of benzyl alcohol in an aqueous methanol solution at 573 K, on. A catalytic process for producing ketones and particularly methyl-benzyl-ketone is provided. A catalyst comprising thorium oxide and a second metal oxide, preferably MnO, is formed on a substrate, preferably pumice. Phenylacetic acid and acetic acid are reacted in the presence of the catalyst to form methyl-benzyl-ketone. An acceptable method is to oxidize methyl benzyl carbinol (l-phenyl-2-propanol) to phenylacetone ( methyl benzyl ketone) with chrome oxide (CrO3) in pyridine solvent. The problem with this is that methyl benzyl carbinol is not commercially available, and so must be made from benzyl chloride grignard reagent and acetaldehyde. SECTION 44-53-210. Schedule II. (a) The controlled substances listed in this section are included in Schedule II. (b) Any of the following substances except those narcotic drugs listed in other schedules whether produced directly or indirectly by extraction from substances of vegetable origin, or independently by means of chemical synthesis, or by combination of extraction and chemical synthesis:.

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Benzyl methyl ketone (BMK) is a well-known amphetamine drug precursor. • The first electrochemical (capacitive) sensor for BMK in water was developed. • Selective molecularly.

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The synthesis [from D(+)-tryptophan] of the tetracyclic ketone [(−)-1b] was carried out in enantiospecifc fashion (>98% ee) via the 1,3-transfer of chirality from N a -methyl, N b -benzyl tryptophan methyl ester [(+)-14] to the trans diastereomer [(−)-4b] in the Pictet-Spengler reaction. Although the condensation of 14 with aldehyde (15) in refluxing benzene generated the tetrahydro β. The detection of benzyl methyl ketone (BMK) is of interest as it is a com-mon precursor for the synthesis of (meth)amphetamine. Resonant gravimetric sensors can be used to detect the mass and hereby the concentration of a gas while colorimetric arrays typically have exceptional selectivities to a target an-alyte. Vinyl alcohol and ehtanal are. When benzyl methyl ketone is allowed to react with ethylene glycol in benzene the product formed is. Which aming the following gives positive iodoform test as well as positive Fehling testAcetophenone. Which ketone will form 3-ethylpentan-3-ol on treatment with ethyl magnesium bromide. thesis describes investigations into the synthesis of the Wieland-Miescher ketone (WMK) analogue 1; an important intermediate in the prospective synthesis of pyrazole 2. The traditional route towards WMK analogues via a Robinson annulation proved to be unsuccessful, with a range of catalysts trialed for the key Robinson annulation step.

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The following procedure was used: 0.484mmol BMK-oxime was dissolved in ethanol and mixed with anaqueous solution of 4.84 mmol EDC. The solution was diluted upto 840 mL with 10 mM phosphate buffer at pH 6 and incubatedfor 20 min at room temperature. A novel whole-cell biocatalyst with high allylic alcohol-oxidizing activities was screened and identified as Yokenella sp. WZY002, which chemoselectively reduced the C=O bond of allylic aldehydes/ketones to the corresponding α,β-unsaturated alcohols at 30°C and pH 8.0. The strain also had the capacity of stereoselectively reducing aromatic ketones to (S).

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  • Phenylacetone (known also as phenylpropan-2-one, benzyl methyl ketone, or methyl benzyl ketone), is an organic compound. It is a clear oil with a refractive index of 1.5168. Phenylacetone is the immediate precursor for clandestine production of amphetamine and methamphetamine. Phenylacetone on anaerobic incubations with rat liver mitochondria.

  • Abbreviation List for SYNTHESIS, SYNLETT, and SynOpen mL milliliter(s) ... BMS borane-methyl sulfide complex BOMBr benzyl bromomethyl ether BOMCl benzyl chloromethyl ether BOPCl bis(2-oxo-3-oxazolidinyl)phosphinic chloride ... MVK methyl vinyl ketone Na2CO3 sodium carbonate Na2SO4 sodium sulfate NaBH4 sodium borohydride.

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  • The U.S. Department of Energy's Office of Scientific and Technical Information.

  • The reaction scheme is in the attached file, but i'll give you rundown... the ketone is formed by the tautomerization of the enol, which is created by hydroboration of the internal alkyne in tetrahydrofuran. The internal alkyne is formed by the alkylation of.

Cyclic ketones have two alpha-carbon atoms, each of which might shift to the nascent 1º-carbocation. If R = H in the case shown here, these two groups are identical and on shifting give the same product. If R = CH 3, the 2º-alkyl group shifts preferentially, the chief product being 3-methylcyclohexanone; the 2-methyl isomer is a minor product. Methyl Sec.-Butyl ketone OR 3-Methyl-2-Pentanone [565-61-7] 95%: ... Specility: 7: 2-Benzyl cyclohexylamine [72436-51-2] 98% : Specility: 8: Dimethyl-5-Sodiosulpho isophthalate [3965-55-7] 99%: Additive in Polyester and nylon fibre synthesis, Intermediate. 9: 5-Lithiosulfo ... Peptide synthesis: 11: 2-Methyl-6-Carboxy-quinolic acid: 99%: Pharma.

Fine Chemicals Product NameCAS No 2-Chloro-3-nitrobenzoic acid3970-35-2 3-nitro 2-acetamido toluene (4-(N-Acetyl) Amino-3-Nitrotoluene)29111-73-7 3-nitro 2-amino toluene570-24-1 3-nitro 2-bromo toluene41085-43-2 3-nitro 2-chloro toluene3970-40-9 3-nitro 2-iodotoluene6277-17-4 2-nitro 6-methyl benzonitrile1885-76-3 2-nitro 6-methyl benzoic acid34545-18-1 2-nitro 6-methyl benzoic acid methyl.

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Ketones, benzyl phenyl synthesis Ketones are oxidatively cleaved by Cr(VI) or Mn(VII) reagents. The reaction is sometimes of utility in the synthesis of difunctional molecules by ring.

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Unless listed in another schedule, any material, compound, mixture, or preparation which contains any quantity of the following substances: (1) Immediate precursor to amphetamine and methamphetamine: (A) Phenylacetone, phenyl-2-propanone(P2P), benzyl methyl ketone, methyl benzyl ketone;. Benzyl ethyl ketone - cas 1007-32-5, synthesis, structure, density, melting point, boiling point. ChemSynthesis Chemical database. ... methyl 11-dodecenoate (29972-79-0) 2-furylmethyl. Phenylacetone is an organic compound with the chemical formula C 6 H 5 CH 2 COCH 3. It is a colorless oil that is soluble in organic solvents. This substance is used in the manufacture of methamphetamine and amphetamine, where it is commonly known as P2P. General procedure for the Synthesis of β-Amino Ketone A mixture of substituted acetophenone (10.0 mmol), N-methylbenzylamine (1.54 mL, 12 mmol), ... alkalified and purified to afford the β-amino ketone. 3-(Benzyl(methyl)amino)-1-phenylpropan-1-one (3a)2.

Benzyl isopropyl ketone | C11H14O | CID 76163 - structure, chemical names, physical and chemical properties, classification, patents, literature, biological.

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Methyl propyl ketone (MPK) or 2-Pentanone is a medium evaporating, urethane-grade solvent. It’s commonly used as a solvent for synthetic resins as well as in gravure printing inks and cleaning and surface preparation applications for the transportation industry. Methyl iodide preparation-ZB7YSR3CaUE.mp4 download. 115.3M ... Preparation of crude benzyl cyanide from benzyl chloride-wD7RbDiqRAU.mp4 download. 81.4M ... Prepare aromatic ketones from calcium benzoate-IzJhi6jkhjI.ogv download. 20.9M. We prepared a series of ordered mesoporous carbons embedded with different contents of Cu nanoparticles (Cu/OMC-X) and applied them to electrocatalytic synthesis of benzyl methyl carbonate.The materials were characterized by many measurements, which showed that Cu/OMC-X materials maintain highly ordered mesoporous structures with high. Benzyl Methyl Ketone supplier. wholesale bmk powder cas 5449-12-7. BMK OIL CAS 20320-59-6. Bikri24. (g) Unless specifically excepted or unless listed in another schedule, any material, compound, mixture, or preparation which contains any quantity of the following substance: (1) Immediate precursor to amphetamine and methamphetamine: (i) Phenylacetone, also known as phenyl-2-propanone; P2P; benzyl methyl ketone; methyl benzyl ketone.

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Starting from methyl acetoacetate and any other necessary reagents, complete the most efficient three-step synthesis of the ketone, 3-benzyl-5-methylhexan-2-one, by dragging the appropriate compound(s) into the boxes. Only one set of reagents will fit. It might be synthesized by the reaction of benzaldehyde and nitroethane inside seeing a basic driving force. In this reaction, the base deprotonates nitroethane to outline a resonation offset anion. This anion nucleophilically adds to the aldehyde confining a beta nitro alcohol, which is thusly got dried out to yield the nitroalkene. Intro The "Wittig Reaction" is one of the premier methods for the synthesis of alkenes. It uses a carbonyl compound as an electrophile, which is attacked by a "phosphorus ylide" (the "Wittig ... or Ketone Alken General Wittig Reaction: Synthesis of Alkenes R Ph3PR 1 The "Wittig Reagent" an "ylide" Base ( usalyBLi) Br + Ph3P=0. Buy Quality Benzyl methyl ketone Online Phenylacetone,is an organic compound.It is a clear oil with a refractive index of 1.5168.This substance.

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Starting from methyl acetoacetate and any other necessary reagents, complete the most efficient three-step synthesis of the ketone, 3-benzyl-5-methylhexan-2-one, by dragging the appropriate compound(s) into the boxes. Only one set of reagents will fit.

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Malonic ester synthesis is a synthetic procedure used to convert a compound that has the general structural formula 1 into a carboxylic acid that has the general structural formula 2. R 1 = alkyl group. L = leaving group. The group —CH 2 CO 2 H in 2 is contributed by a malonic ester, hence the term malonic ester synthesis. The methyl vinyl ketone annelation of pyrrolines was extended to an erythrinan synthesis (679). Perhydrophenan-threnones were obtained from 1-acetylcyclohexene and pyrrolidinocyclo-hexene (680) or alternatively from Birch reduction and cyclization of a 2- pyridyl ethyl ketone intermediate, which was formed by alkylation of an enamine with a 2. Description. ENQUIRY. Phenylacetone ( also known as 2-phenyl-2one, benzyl menthyl methyl ketone, or benzyl-ketone bromide), is an organic compound. It .is clear oil with a refractive index of 1.5168. This Sunstance in the manufacture of methaphetamine and amphetamine asa raw material or intermidiate, where it is commonly referred to as P2P as. China Dimethyl Benzyl Carbinol manufacturers - Select 2022 high quality Dimethyl Benzyl Carbinol products in best price from certified Chinese Dimethyl, Dimethyl Ether suppliers, wholesalers and factory on Made-in-China.com.

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Industrial acetophenone major impurities are alpha-methyl benzyl alcohol, phenol, acids, and water, purified using calcium chloride or sulfate fractionation decompression after drying. Or avoid light and Humidity circumstances, from the molten state of fractional crystallization refined, can also be used in low-temperature crystal Pentane refined. Protecting Groups for Aldehydes and Ketones (Acetal and Ketal Protecting Groups) Formation ... Methyl Esters R C OCH ... The common ester protecting groups for carboxylic acids are methyl, ethyl and benzyl esters. 1:56 PM. Protecting Groups for Carboxylic Acids (Esters) Ethyl and benzyl esters are prepared based on the following rationale: 22.

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The reaction mass is heated for 1.5 h at 90-100 C, another 60 l of water is added and methyl benzyl ketone is extracted with chloroform. To chloroform extracts (about 20 kg) add 17 kg of. This article describes the synthesis of 4,5-disubstitued 2-aminothiazolium hydrochloride salts. The method is exemplified in the synthesis of 2-aminothiazole 3 from a readily available enone. High yields of 5-benzyl-4-methyl-2-aminothiazolium hydrochloride are obtained in 3 steps, avoiding difficult or expensive purifications.

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The following procedure was used: 0.484mmol BMK-oxime was dissolved in ethanol and mixed with anaqueous solution of 4.84 mmol EDC. The solution was diluted upto 840 mL with 10 mM.